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Water Resistant Mascara with LUXSIL

Formulation

Water Resistant Mascara with LUXSIL

NameIngredientSupplier%
Phase A
Deionized Water
Water
Water62.40
Methylparaben, USP
Methylparaben
MethylparabenISP0.25
Keltrol
Xanthan Gum
Xanthan GumKelco0.50
PVP K-30
PVP
PVPISP2.00
Luxsil®
Calcium Aluminum Borosilicate
Calcium Aluminum BorosilicatePresperse, Inc.2.00
Black Iron Oxide C33-7774
Iron Oxide
Iron OxideSun Chemical7.00
Ultramarine Blue 7104
Ultramarines
UltramarinesWarner Jackenson0.10
Triethanolamine 99%
Triethanolamine
TriethanolamineUnion Carbide1.00
Lipo PE Base G-55
Glycerin (and) Diglycol/CHDM/Isophthalates/SIP Copolymer
Glycerin (and) Diglycol/CHDM/Isophthalates/SIP CopolymerLipo Chemicals8.00
Phase C
Deionized Water
Water
Water1.00
Germall 115
Imidazolidinyl Urea
Imidazolidinyl UreaISP0.30
Phase B
Carnauba Wax
Carnauba
CarnaubaStrahl & Pitsch Inc.4.00
Beeswax (White)
Beeswax
BeeswaxHansotech Inc.4.00
Permethyl® 104A
Polyisobutene
PolyisobutenePresperse, Inc.4.00
Emersol 132
Stearic Acid
Stearic AcidHenkel/Chemical Group2.50
Lipo GMS 450
Glyceryl Stearate
Glyceryl StearateLipo Chemical1.00
Propylparaben, USP
Propylparaben
PropylparabenISP0.20

Preparation: Procedure 1. In a suitable kettle, slowly add xanthan gum into the vortex of water, using a low shear agitation. Disperse completely. 2. Pre-mix the remaining powder ingredients of Phase A in a blender type until the colour pigments are completely dispersed. 3. Start heating the batch to 60°–70°C. Then add the pre-mixed pigments and the remaining ingredients of Phase A into the batch. 4. Mix well every each ingredient addition. Hold the temperature while the batch is constantly mixing. 5. After ten minutes of mixing, pass Phase A into homomixer and homogenize the batch for 5 minutes or until uniformly dispersed. 6. Change the mixing into propeller mixing and bring up the temperature to 80°–84°C. 7. In a separate kettle, combine Phase B materials and heat to 80°–84°C. 8. When both Phases are at the same temperature, add Phase B to Phase A applying moderate agitation. 9. Start cooling at 45°–40°C. Add the premixed Phase C into the batch. 10. Continue mixing until it reaches to 35°–30°C. 11. Pour into appropriate containers.